3,5-Dinitrobenzoyl chloride

3,5-Dinitrobenzoyl chloride Structure
3,5-Dinitrobenzoyl chloride structure
Common Name 3,5-Dinitrobenzoyl chloride
CAS Number 99-33-2 Molecular Weight 230.562
Density 1.7±0.1 g/cm3 Boiling Point 339.0±22.0 °C at 760 mmHg
Molecular Formula C7H3ClN2O5 Melting Point 68-69 °C(lit.)
MSDS Chinese USA Flash Point 158.8±22.3 °C
Symbol GHS05
GHS05
Signal Word Danger

Refinements to the structure of graphite oxide: absolute quantification of functional groups via selective labelling.

Nanoscale 7 , 20256-66, (2015)

Chemical modification and functionalization of inherent functional groups within graphite oxide (GO) are essential aspects of graphene-based nano-materials used in wide-ranging applications. Despite extensive research, there remains some discrepancy in its st...

Liquid chromatographic determination of biogenic amines in fermented foods after derivatization with 3,5-dinitrobenzoyl chloride.

J. Chromatogr. A. 881(1-2) , 517-30, (2000)

The reagent 3,5-dinitrobenzoyl chloride (DNBZ-Cl) was tested for pre-column derivatization of biogenic amines (BAs). Samples were derivatized within 3 min in 1 M NaOH at ambient temperature by adding 2-propanole and 50 mM DNBZ-Cl in acetonitrile. The reaction...

Bombesin stimulates distinct time-dependent changes in the sn-1,2-diradylglycerol molecular species profile from Swiss 3T3 fibroblasts as analysed by 3,5-dinitrobenzoyl derivatization and h.p.l.c. separation.

Biochem. J. 289 , 487, (1993)

We have developed procedures for the analysis of endogenous diradylglycerol (DRG) molecular species using derivatization with 3,5-dinitrobenzoyl chloride. The introduction of this strong chromatophore enabled us to separate less than 1 nmol of DRG into its th...

Common filaggrin gene mutations and risk of cervical cancer.

Acta Oncol. 54(2) , 217-23, (2015)

As carriers of filaggrin gene (FLG) mutations may have a compromised cervical mucosal barrier against human papillomavirus infection, our primary objective was to study their risk of cervical cancer.We genotyped 586 cervical cancer patients for the two most c...

Synthetic analogues of netropsin and distamycin. IV. Synthesis of a new carbocyclic analogue of distamycin with alkylating side groups.

Rocz. Akad. Med. Bialymst. 42(1) , 129-40, (1997)

A carbocyclic analogue of distamycin was obtained, in which the N-methylpyrrole rings were substituted by disubstituted benzene rings. Additionally, N-chloro- or N-bromoacetyl groups, displaying alkylating properties, were introduced. The synthesis, starting ...

HPLC analysis of polyamines and their acetylated derivatives in the picomole range using benzoyl chloride and 3,5-dinitrobenzoyl chloride as derivatizing agent.

Biomed. Chromatogr. 2(6) , 254-7, (1988)

Analytical methods are described for the quantitative determination of putrescine, cadaverine, spermidine, spermine and the acetylated derivatives of spermidine and spermine in biological fluids using pre-column derivatization with either benzoyl chloride or ...

[Synthesis of a novel starch derivative and its adsorption property for creatinine].

Yao Xue Xue Bao 38(3) , 191-5, (2003)

To prepare a novel creatinine adsorbent with anti-renal failure activity.A novel starch ester was prepared under heterogeneous condition by the reaction of starch (ST) and 3, 5-dinitrobenzoyl chloride (DNBZ-Cl). The products were characterized by means of ele...

High-performance liquid chromatographic determination of taurine and hypotaurine using 3,5-dinitrobenzoyl chloride as derivatizing reagent.

J. Chromatogr. B, Biomed. Appl. 660(1) , 31-5, (1994)

A method for the determination of taurine and hypotaurine in biological samples involving the preparation of their 3,5-dinitrobenzoyl derivatives followed by HPLC was established. Taurine and hypotaurine in aqueous media were reacted with 3,5-dinitrobenzoyl c...

Liquid chromatographic analysis of amphetamine and related compounds in urine using solid-phase extraction and 3,5-dinitrobenzoyl chloride for derivatization.

J. Chromatogr. Sci. 35(4) , 169-75, (1997)

A chromatographic method for the analysis of amphetamine and related compounds in urine using 3,5-dinitrobenzoyl chloride (3,5-DNB) as a labeling reagent is presented. This assay is based on the employment of solid-phase extraction (SPE) cartridges for sample...

Studies on neurosteroids XXIII. Analysis of tetrahydrocorticosterone isomers in the brain of rats exposed to immobilization using LC-MS.

Steroids 72 , 865-874, (2007)

The identification and quantification of tetrahydrocorticosterone isomers (THBs; 3alpha,5alpha-, 3beta,5alpha-, 3alpha,5beta- and 3beta,5beta-THB) in rat brains using liquid chromatography (LC)-mass spectrometry (MS) are described. For the identification, the...