4′-Chloroacetoacetanilide

Modify Date: 2025-08-21 08:10:22

4′-Chloroacetoacetanilide Structure
4′-Chloroacetoacetanilide structure
 Common Name 4′-Chloroacetoacetanilide
CAS Number 101-92-8 Molecular Weight 211.645
Density 1.3±0.1 g/cm3 Boiling Point 400.5±30.0 °C at 760 mmHg
Molecular Formula C10H10ClNO2 Melting Point 131-134 °C(lit.)
MSDS Chinese USA Flash Point 196.0±24.6 °C

 Use of 4′-Chloroacetoacetanilide


AI3-17671 is a biochemical.

 Names

Name 4'-Chloroacetoacetanilide
Synonym More Synonyms

 Chemical & Physical Properties

Density 1.3±0.1 g/cm3
Boiling Point 400.5±30.0 °C at 760 mmHg
Melting Point 131-134 °C(lit.)
Molecular Formula C10H10ClNO2
Molecular Weight 211.645
Flash Point 196.0±24.6 °C
Exact Mass 211.040009
PSA 46.17000
LogP 1.82
Vapour Pressure 0.0±0.9 mmHg at 25°C
Index of Refraction 1.579

 Toxicological Information

CHEMICAL IDENTIFICATION

RTECS NUMBER :
AK4375000
CHEMICAL NAME :
Acetoacetanilide, 4'-chloro-
CAS REGISTRY NUMBER :
101-92-8
BEILSTEIN REFERENCE NO. :
1819161
LAST UPDATED :
199701
DATA ITEMS CITED :
2
MOLECULAR FORMULA :
C10-H10-Cl-N-O2
MOLECULAR WEIGHT :
211.66
WISWESSER LINE NOTATION :
GR DMV1V1

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :
LDLo - Lowest published lethal dose
ROUTE OF EXPOSURE :
Intraperitoneal
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
500 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
REFERENCE :
CBCCT* "Summary Tables of Biological Tests," National Research Council Chemical-Biological Coordination Center. (National Academy of Science Library, 2101 Constitution Ave., NW, Washington, DC 20418) Volume(issue)/page/year: 4,225,1952

 Safety Information

Personal Protective Equipment Eyeshields;Gloves;type N95 (US);type P1 (EN143) respirator filter
Hazard Codes Xi
Safety Phrases S24/25
RIDADR NONH for all modes of transport
WGK Germany 1
RTECS AK4375000
HS Code 2924299090

 Synthetic Route

3-(4-CHLORO-PHENYL)-6-METHYL-[1,3]OXAZINE-2,4-DIONE structure

3-(4-CHLORO-PHE...

CAS#:30645-78-4

~52%

4′-Chloroacetoacetanilide Structure

4′-Chloroacetoa...

CAS#:101-92-8

Literature: Chemical and Pharmaceutical Bulletin, , vol. 37, # 8 p. 2026 - 2029
3-(4-chlorophenylamino)-2-[(4-chlorophenylimino)methyl]acrylonitrile structure

3-(4-chlorophen...

CAS#:1352630-23-9

2,2,6-Trimethyl-4H-1,3-dioxin-4-one structure

2,2,6-Trimethyl...

CAS#:5394-63-8

~0%

4′-Chloroacetoacetanilide Structure

4′-Chloroacetoa...

CAS#:101-92-8

5-acetyl-1-(4-chlorophenyl)-6-oxo-1,6-dihydropyridine-3-carbonitrile structure

5-acetyl-1-(4-c...

CAS#:1352630-35-3

Literature: European Journal of Organic Chemistry, , # 30 p. 6085 - 6091
Ethyl acetoacetate structure

Ethyl acetoacetate

CAS#:141-97-9

4-Chloroaniline structure

4-Chloroaniline

CAS#:106-47-8

~68%

4′-Chloroacetoacetanilide Structure

4′-Chloroacetoa...

CAS#:101-92-8

Literature: Journal of Chemical Sciences, , vol. 126, # 1 p. 187 - 195
Diketene structure

Diketene

CAS#:674-82-8

4-Chloroaniline structure

4-Chloroaniline

CAS#:106-47-8

~%

4′-Chloroacetoacetanilide Structure

4′-Chloroacetoa...

CAS#:101-92-8

Literature: Collection of Czechoslovak Chemical Communications, , vol. 50, # 2 p. 365 - 374
3-(4-CHLORO-PHENYL)-6-METHYL-[1,3]OXAZINE-2,4-DIONE structure

3-(4-CHLORO-PHE...

CAS#:30645-78-4

2-Aminoethanol structure

2-Aminoethanol

CAS#:141-43-5

~18%

4′-Chloroacetoacetanilide Structure

4′-Chloroacetoa...

CAS#:101-92-8

3-(4-Chlorophenyl)-1-(2-hydroxyethyl)-6-methyl-2,4(1H,3H)-pyrimidinedione structure

3-(4-Chlorophen...

CAS#:126401-63-6

Literature: Chemical and Pharmaceutical Bulletin, , vol. 37, # 8 p. 2026 - 2029
2,2,6-Trimethyl-4H-1,3-dioxin-4-one structure

2,2,6-Trimethyl...

CAS#:5394-63-8

4-Chloroaniline structure

4-Chloroaniline

CAS#:106-47-8

~53%

4′-Chloroacetoacetanilide Structure

4′-Chloroacetoa...

CAS#:101-92-8

Literature: Synthetic Communications, , vol. 38, # 23 p. 4226 - 4239
Diketene structure

Diketene

CAS#:674-82-8

Carbamodithioic acid,N-(4-chlorophenyl)-, ammonium salt (1:1) structure

Carbamodithioic...

CAS#:1197-56-4

~%

4′-Chloroacetoacetanilide Structure

4′-Chloroacetoa...

CAS#:101-92-8

Literature: Archiv der Pharmazie (Weinheim, Germany), , vol. 314, # 7 p. 587 - 594
Pyridine structure

Pyridine

CAS#:110-86-1

Carbon tetrachloride structure

Carbon tetrachloride

CAS#:56-23-5

Ethyl acetoacetate structure

Ethyl acetoacetate

CAS#:141-97-9

4-Chloroaniline structure

4-Chloroaniline

CAS#:106-47-8

~%

Detail
Literature: Gazzetta Chimica Italiana, , vol. 66, p. 723,727

 Customs

HS Code 2924299090
Summary 2924299090. other cyclic amides (including cyclic carbamates) and their derivatives; salts thereof. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:30.0%

 Articles3

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Preparation of 4-anilino-6-aryl-2 H-pyran-2-ones from trilithiated acetoacetanilides and aromatic esters. Downs JR, et al.

Can. J. Chem. 82(5) , 659-664, (2004)

Synthesis and antimicrobial activity of n, 7-diaryl-5-methyl-4, 7-dihydrotetrazolo [1, 5-a] pyrimidine-6-arboxamides. Gein VL, et al.

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 Synonyms

4‘-Chloroacetoacetanilide
4'-Chloroacetoacetan
GR DMV1V1
N-(4-Chlorphenyl)-3-oxobutanamide
3-oxo-N-(4'-chlorophenyl)butanamide
MFCD00000613
N-(4-Chlorophenyl)acetoacetamide
N-(4-methoxyphenyl)-3-oxobutanamide
p-Acetoacetchloranilide
Acetoacetanilide, 4'-chloro-
P-CHLOROACETOACETANILIDE
Butanamide, N-(4-chlorophenyl)-3-oxo-
N-Acetoacetyl-4-chloroaniline
PARA-CHLOROACETOANILIDE
Acetoacetanilide, p-chloro-
EINECS 202-989-6
N-(4-Chlorophenyl)-3-oxobutanamide
AAPCA
N-(4-chlorophenyl)-3-oxobutyramide
Acetoacet-p-chloroanilide
4′-Chloroacetoacetanilide
4'-Chloroacetoacetanilide
p-chlorodiacetanilide
4'-CHLOROACETACETANILIDE
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