Tetrahedron Letters

A class of new silylating agents. II. A highly reactive reagent for introduction of the trimethylsilyl group.

T Veysoglu, LA Mitscher

文献索引：Veysoglu, Tarik; Mitscher, Lester A. Tetrahedron Letters, 1981 , vol. 22, # 14 p. 1303 - 1306

被引用次数: 22

摘要

Download full text in PDF Opens in a new window. Article suggestions will be shown in a dialog on return to ScienceDirect. ... Please enable JavaScript to use all the features on this page. ... Trimethylsilyl enol ethers of pentane-2,4-dione and methyl acetoacetate react rapidly with alcohols at room temperature without the need for catalytic assistance to give high isolated yields of trimethylsilyl ethers. ... The reactions were monitored and purity was established in all cases using a ...

~82%

~86%

~81%

A novel, chemoselective and efficient microwave-assisted dep...

[Saxena, Ira; Deka, Nabajyoti; Sarma, Jadab C.; Tsuboi, Sadao Synthetic Communications, 2003 , vol. 33, # 23 p. 4005 - 4011]

Efficient O-trimethylsilylation of alcohols and phenols with...

[Amantini; Fringuelli; Pizzo; Vaccaro Journal of Organic Chemistry, 2001 , vol. 66, # 20 p. 6734 - 6737]

Mild and practical method for the silylation of alcohols usi...

[Tanabe, Yoo; Okumura, Hitomi; Maeda, Akihiro; Murakami, Masanari Tetrahedron Letters, 1994 , vol. 35, # 45 p. 8413 - 8414]

Counterattack reagent hexamethyldisilane in the direct conve...

[Hwu, Jih Ru; Lin, Lung Ching; Liaw, Ben Ruey Journal of the American Chemical Society, 1988 , vol. 110, # 21 p. 7252 - 7254]

Efficient O-trimethylsilylation of alcohols and phenols with...

[Kita,Y. et al. Tetrahedron Letters, 1979 , p. 4311 - 4314]