e.g. Filippa Pettersson or Cancer Res. 75(6) , 1102-12, (2015) or 10.1002/anie.201600521

Tetrahedron

Quantitative solid-state reactions of amines with carbonyl compounds and isothiocyanates

G Kaupp, J Schmeyers, J Boy

Index: Kaupp, Gerd; Schmeyers, Jens; Boy, Juergen Tetrahedron, 2000 , vol. 56, # 36 p. 6899 - 6911

Full Text: HTML

Citation Number: 66

Abstract

A series of solid-state reactions is reported of gaseous or solid amines with aldehydes to give imines, with solid anhydrides to give diamides (therefrom imides) or amidic carboxylic salts or imides, with solid imides to give diamides, with solid lactones or carbonates to give functionalized carbamic esters, with polycarbonates to give degradative aminolysis, and with solid isothiocyanates to give thioureas. Diamides give imides by solid-state thermolysis or ...

4-Nitrophenyl isothiocyanate Structure

4-Nitrophenyl i...

methylamine Structure

~99%

1-methyl-3-(4-nitrophenyl)thiourea Structure

1-methyl-3-(4-n...

Ethylamine Structure

4-bromophenyl isothiocyanate Structure

4-bromophenyl i...

~99%

3-(4-bromophenyl)-1,1-dimethylthiourea Structure

3-(4-bromopheny...

methylamine Structure

4-bromophenyl isothiocyanate Structure

4-bromophenyl i...

~99%

1-(4-Bromophenyl)-3-methylthiourea Structure

1-(4-Bromopheny...

Methyl isothiocyanate Structure

Methyl isothioc...

4-Bromoaniline Structure

~99%

1-(4-Bromophenyl)-3-methylthiourea Structure

1-(4-Bromopheny...

Ethylamine Structure

Methyl isothiocyanate Structure

Methyl isothioc...

~99%

trimethylthiourea Structure

trimethylthiourea

phthalimide Structure

methylamine Structure

~99%

1,2-Benzenedicarboxamide, N,N'-dimethyl- Structure

1,2-Benzenedica...

N-Hydroxyphthalimide Structure

N-Hydroxyphthalimide

methylamine Structure

~99%

1,2-Benzenedicarboxamide, N,N'-dimethyl- Structure

1,2-Benzenedica...

N-Phthaloylglycine Structure

N-Phthaloylglycine

methylamine Structure

~99%

1,2-Benzenedicarboxamide, N,N'-dimethyl- Structure

1,2-Benzenedica...

N,N'-diethylphthalic diamide Structure

N,N'-diethylpht...

methylamine Structure

~%

1,2-Benzenedicarboxamide, N,N'-dimethyl- Structure

1,2-Benzenedica...

phthalimide Structure

~%

1,2-Benzenedicarboxamide, N,N'-dimethyl- Structure

1,2-Benzenedica...

N-Hydroxyphthalimide Structure

N-Hydroxyphthalimide

~%

1,2-Benzenedicarboxamide, N,N'-dimethyl- Structure

1,2-Benzenedica...

n-ethylphthalimide Structure

n-ethylphthalimide

~%

1,2-Benzenedicarboxamide, N,N'-dimethyl- Structure

1,2-Benzenedica...

N-Phthaloylglycine Structure

N-Phthaloylglycine

~%

1,2-Benzenedicarboxamide, N,N'-dimethyl- Structure

1,2-Benzenedica...

N,N'-diethylphthalic diamide Structure

N,N'-diethylpht...

~98%

n-ethylphthalimide Structure

n-ethylphthalimide

Glutarimide Structure

Dimethylamine Structure

~99%

N',N'-dimethylpentanediamide Structure

N',N'-dimethylp...

4-Nitrobenzaldehyde Structure

4-Nitrobenzaldehyde

Ethylamine Structure

~97%

N-ethyl-1-(4-nitrophenyl)methanimine Structure

N-ethyl-1-(4-ni...

Phenyl isothiocyanate Structure

Phenyl isothioc...

~99%

Phenylthiocarbamide Structure

Phenylthiocarbamide

Formaldehyde Structure

L-cysteine Structure

~98%

L-Thioproline Structure

4-Chloroaniline Structure

4-Chloroaniline

Methyl isothiocyanate Structure

Methyl isothioc...

~99%

1-(4-chlorophenyl)-3-methylthiourea Structure

1-(4-chlorophen...

Phthalic anhydride Structure

Phthalic anhydride

p-Toluidine Structure

~97%

2-P-TOLYL-ISOINDOLE-1,3-DIONE Structure

2-P-TOLYL-ISOIN...

Efficient conversion of substituted aryl thioureas to 2-amin...

[Ambati, Narahari Babu; Anand; Hanumanthu Synthetic Communications, 1997 , vol. 27, # 9 p. 1487 - 1493]