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Continuous organomagnesium synthesis of organometallic compounds

PA Storozhenko, AA Grachev, AO Klochkov…

文献索引:Storozhenko; Grachev; Klochkov; Shiryaev Russian Journal of Applied Chemistry, 2013 , vol. 86, # 3 p. 387 - 393

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摘要

Abstract Continuous organomagnesium synthesis of a number of organic derivatives of 14th group elements of the periodic table was examined in a column apparatus with an agitator. An effect of a molar ratio of reactants, temperature in a reaction zone, and other factors was studied on the yield and composition of the products.