High??Yielding Cleavage of (Aryloxy) acetates

A Spurg, SR Waldvogel

文献索引：Spurg, Anke; Waldvogel, Siegfried R. European Journal of Organic Chemistry, 2008 , # 2 p. 337 - 342

被引用次数: 11

摘要

Abstract A reliable and high-yielding one-pot sequence for the removal of O-carboxymethyl moieties from phenols is presented. When diethylphosphoryl azide is employed as theazide transfer reagent in the Curtius rearrangement and glycerol in the subsequent hydrolytic workup, the protocol can be reliably applied to a very broad scope of substrates.(© Wiley- VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2008)

~49%

5348-75-4

2-([1,1'-联苯]-2-...

~81%

~79%

~45%

~10%

~67%

~95%

~86%

~85%

~67%

~85%

~89%

~72%

~90%

~75%

~87%

~98%

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