Synthetic communications

A practical synthesis of Np-anisyl-N-methyl-amino-3-(9-anthryl)-propane: An exciplex fluorescence 'thermometer'

AC Spivey, AJ Bissell, B Stammen

文献索引：Spivey, Alan C.; Bissell, Andrew J.; Stammen, Blanda Synthetic Communications, 1998 , vol. 28, # 4 p. 623 - 632

被引用次数: 4

摘要

Abstract A practical synthesis of Np-anisyl-N-methyl-amino-3-(9-anthryl)-propane from 9- anthraldehyde is described. All the intermediates in this simple five step sequence are crystalline and simple re-crystallisation after each step allows the preparation of this exciplex fluorescence 'thermometer'molecule on a preparative scale without resort to chromatography.

~90%

~85%

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