The Journal of Organic Chemistry

Thiolesters. Reaction of Thiols with Acrylyl and Crotonyl Chlorides

AA Schleppnik, FB Zienty

文献索引：Schleppnik,A.A.; Zienty,F.B. Journal of Organic Chemistry, 1964 , vol. 29, p. 1910 - 1915

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被引用次数: 13

摘要

An improved method is described for preparation of thiolcrotonates by reaction of crotonyl chloride with thiols. General convenient and high-yield methods of making the new dl-3- chlorothiolbutyrates and the new dl-3-alkyl (aryl) thiothiolbutyrates involve addition of hydrogen chloride and of thiols, respectively, to thiolcrotonates. General procedures for making thiolesters by esterification of thiols with anhydride8 involve use of 1 mole of ...