Journal of the American Chemical Society

STUDIES ON POLYMERIZATION AND RING FORMATION. XVII. FRIEDEL-CRAFTS SYNTHESES WITH THE POLYANHYDRIDES OF THE DIBASIC ACIDS

JW Hill

文献索引：Hill Journal of the American Chemical Society, 1932 , vol. 54, p. 4105

全文：HTML全文

被引用次数: 15

摘要

4106 JULIAN W. HILL Vol. 54 anhydride for six hours. The excess acetic anhydride and the acetic acid formed in the reaction were removed by distillation in vacuo up to 120 O bath temperature. The resulting polyanhydride" was dissolved in 400 cc. of warm, dry benzene. Three hundred grams of anhydrous aluminum chloride was suspended in 1500 cc. of dry benzene contained in a 3-necked 3-liter flask fitted with a reflux condenser and a ...