Chemistry letters

Reduction with Samarium (0). Debromination of vic-Dibromides to Alkenes.

R Yanada, K Bessho, K Yanada

Index: Yanada, Reiko; Bessho, Kiyoshi; Yanada, Kazuo Chemistry Letters, 1994 , # 7 p. 1279 - 1282

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Citation Number: 27

Abstract

Three electrons from Sm (0) to Sm (III) can be available during the title reduction which was achieved in 90–95% yield with vic-dibromides such as trans-10, 11- dibromodibenzosuberone, meso-and dl-1, 2-dibromo-1, 2-diphenylethane, ethyl 2, 3- dibromo-3-phenylpropionate, 2, 3-dibromo-3-phenylpropionic acid, and cholesterol dibromide. These reductions were accelerated with a catalytic amount of acid.

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