Phosphorus Compounds. II. Synthesis of Unsymmetrical Tertiary Phosphines1, 2
WJ BAILEY, SA BUCKLER…
Index: Bailey,W.J. et al. Journal of Organic Chemistry, 1960 , vol. 25, p. 1996 - 2000
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Citation Number: 20
Abstract
The reduction of benzyl-containing phosphonium compounds with lithium aluminum hydride has been used for the synthesis of two unsymmetrical tertiary phosphines. Thus et hylmethylphenylphosphine was prepared from dichlorophenylphosphine in an over-all yield of 5954. Similarly, ethylmethylpentylphosphine was prepared from dichloromethylphosphine in an over-all yield of 507,.
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