The Journal of Organic Chemistry

Mild fluorofunctionalization of side chains in alkyl substituted aromatics by cesium fluoroxysulfate

S Stavber, M Zupan

Index: Stavber, Stojan; Zupan, Marko Journal of Organic Chemistry, 1991 , vol. 56, # 26 p. 7347 - 7350

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Citation Number: 18

Abstract

[lit.21 [cx]~~D -48.8' (C 2, CHCl,)]; 'H NMR 7.42-7.27 (m, 5 H), 5.52 (d, J = 4.9 Hz, 1 H), 5.50-5.40 (m, 1 HI, 5.11 (9, 2 H), 4.63 (dd, J = 8.1, 2.3 Hz, 1 H), 4.36 (dd, J = 8.1, 1.6 Hz, 1 H), 4.31 (dd, J = 4.9, 2.3 Hz, 1 H), 4.11 (bd, J = 6.0 Hz, 1 HI, 3.90-3.70 (m, 3 H), 1.58 (s,3 H), 1.51 (s,3 H), 1.43 (s, 3 H), 1.32 (8, 3 H); 13C NMR 156.8, 136.8, 128.9, 128.5,109.9, 109.3,96.9, 71.4, 71.2, ... Anal. Calcd for CZ1HmNO8: C, 59.56; H, 6.90; N, 3.31. Found C, 59.48; H, 6.75; N, 3.28. ...