Addition d'iodoperfluoroalcanes RFI (C n F 2n+ 1, n= 4, 6, 8) au 2-méthyl-3-butyn-2-ol catalysée par le zinc dans différent solvants. Application à la synthèse de l' …

B Abou-Ghazaleh, P Laurent, H Blancou…

Index: Abou-Ghazaleh, B.; Laurent, Ph.; Blancou, H.; Commeyras, A. Journal of Fluorine Chemistry, 1994 , vol. 68, # 1 p. 21 - 24

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Citation Number: 13

Abstract

Abstract The addition of perfluoroalkyl iodides (RFI) to 2-methyl-3-butyn-2-ol activated by suspended zinc dust has been studied in different solvents and found to lead readily to perfluoroalkene iodides. The latter when treated with a base gave a perfluoroalkyne, RFC CH.

 Related Synthetic Route
5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluoro-2-methyldodec-3-yn-2-ol Structure

84201-71-8

5,5,6,6,7,7,8,8...

~87%

3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodec-1-yne Structure

55009-88-6

3,3,4,4,5,5,6,6...

Perfluorooctyl iodide Structure

507-63-1

Perfluorooctyl ...

~%

3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodec-1-yne Structure

55009-88-6

3,3,4,4,5,5,6,6...

Perfluorobutyl iodide Structure

423-39-2

Perfluorobutyl ...

3-Methyl butynol Structure

115-19-5

3-Methyl butynol

~88%

5,5,6,6,7,7,8,8,8-nonafluoro-3-iodo-2-methyloct-3-en-2-ol Structure

144295-00-1

5,5,6,6,7,7,8,8...

5,5,6,6,7,7,8,8,8-nonafluoro-3-iodo-2-methyloct-3-en-2-ol Structure

144295-00-1

5,5,6,6,7,7,8,8...

~89%

5,5,6,6,7,7,8,8,8-nonafluoro-2-methyloct-3-yn-2-ol Structure

82721-68-4

5,5,6,6,7,7,8,8...

3-Methyl butynol Structure

115-19-5

3-Methyl butynol

~%

5,5,6,6,7,7,8,8,8-nonafluoro-2-methyloct-3-yn-2-ol Structure

82721-68-4

5,5,6,6,7,7,8,8...

5,5,6,6,7,7,8,8,8-nonafluoro-2-methyloct-3-yn-2-ol Structure

82721-68-4

5,5,6,6,7,7,8,8...

~93%

3,3,4,4,5,5,6,6,6-nonafluorohex-1-yne Structure

59665-30-4

3,3,4,4,5,5,6,6...

5,5,6,6,7,7,8,8,8-nonafluoro-3-iodo-2-methyloct-3-en-2-ol Structure

144295-00-1

5,5,6,6,7,7,8,8...

~%

3,3,4,4,5,5,6,6,6-nonafluorohex-1-yne Structure

59665-30-4

3,3,4,4,5,5,6,6...

5,5,6,6,7,7,8,8,9,9,10,10,10-tridecafluoro-3-iodo-2-methyldec-3-en-2-ol Structure

87617-31-0

5,5,6,6,7,7,8,8...

~94%

5,5,6,6,7,7,8,8,9,9,10,10,10-tridecafluoro-2-methyl-dec-3-yn-2-ol Structure

82721-70-8

5,5,6,6,7,7,8,8...

1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-6-iodohexane Structure

355-43-1

1,1,1,2,2,3,3,4...

~%

5,5,6,6,7,7,8,8,9,9,10,10,10-tridecafluoro-2-methyl-dec-3-yn-2-ol Structure

82721-70-8

5,5,6,6,7,7,8,8...

3-Methyl butynol Structure

115-19-5

3-Methyl butynol

~%

5,5,6,6,7,7,8,8,9,9,10,10,10-tridecafluoro-2-methyl-dec-3-yn-2-ol Structure

82721-70-8

5,5,6,6,7,7,8,8...

5,5,6,6,7,7,8,8,9,9,10,10,10-tridecafluoro-2-methyl-dec-3-yn-2-ol Structure

82721-70-8

5,5,6,6,7,7,8,8...

~92%

1H-Perfluorooct-1-yne Structure

55756-24-6

1H-Perfluorooct...


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