Synthetic Communications

Reaction of 2-Naphthylamine with Sodium Iodate/Sodium Sulfite: Synthesis of 2-Amino-1-iodonaphthalene

T Taldone, D Zatorska, G Chiosis

Index: Taldone, Tony; Zatorska, Danuta; Chiosis, Gabriela Synthetic Communications, 2012 , vol. 42, # 5 p. 635 - 638

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Abstract

The reaction of 2-naphthylamine with NaIO 3 /Na 2 SO 3 /HCl yields exclusively 2-amino-1-iodonaphthalene and not regioisomer 2-amino-3-iodonaphthalene as was previously reported. The assigned structure is supported by spectroscopic data. ... The reaction of 2-naphthylamine with NaIO 3 /Na 2 SO 3 /HCl yields exclusively 2-amino-1-iodonaphthalene and not regioisomer 2-amino-3-iodonaphthalene as was previously reported. The assigned structure is supported by spectroscopic data.