Electrochemical reactions of organic sulfides in anhydrous hydrogen fluoride have received some attention in recent years.'This work extends these investigations to include hexyl and phenyl sulfide. As in previous work, the compounds RfSFI,(Rf) &3F4, R, F and Rf-Rf (where R, is C6F13 or cyclo C6F11) were isolated or detected. The yields of isolable product were lorn for phenyl sulfide. Many of the above products that xere liquids at 25" were purified by ...