... The first change (313 to 329 K) takes place where no thermal anomaly is observed in Figs 1-3. However, the ... D .... .1,“ on“ J- WW :0 °¢sn'““ m=l0.7mg Heat flow (mW) ' | 1' I | 1 I | I ' 1' | 300 3 ... DSC curves for m=1l mg and three scanning rates, I/=3, S and 10 K min-1 J. Therm Anal. ...