The Journal of organic chemistry

Stable TEMPO and ABNO Catalyst Solutions for User-Friendly (bpy) Cu/Nitroxyl-Catalyzed Aerobic Alcohol Oxidation

JE Steves, SS Stahl

Index: Wang, Guangjun; Li, Zhengwei; Ha, Chengyong; Ding, Ke Synthetic Communications, 2008 , vol. 38, # 10 p. 1629 - 1637

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Citation Number: 3

Abstract

... 50 mmol reactions should be performed with 250–500 mL MeCN in a 1–2 L round-bottom flask. Large scale reactions should be concentrated in vacuo to ∼10% of the original volume prior to performing purification as described below. ...

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