The Journal of organic chemistry

Stable TEMPO and ABNO Catalyst Solutions for User-Friendly (bpy) Cu/Nitroxyl-Catalyzed Aerobic Alcohol Oxidation

JE Steves, SS Stahl

文献索引：Wang, Guangjun; Li, Zhengwei; Ha, Chengyong; Ding, Ke Synthetic Communications, 2008 , vol. 38, # 10 p. 1629 - 1637

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被引用次数: 3

摘要

... 50 mmol reactions should be performed with 250–500 mL MeCN in a 1–2 L round-bottom flask. Large scale reactions should be concentrated in vacuo to ∼10% of the original volume prior to performing purification as described below. ...

~74%

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~85%

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~93%

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~80%

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~77%

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~71%

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~79%

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~77%

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~63%

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~70%

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~12%

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~83%

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~51%

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~80%

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~79%

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