Synthesis of Alkyl Isothiocyanates from Primary Alkyl Amines using Dicyandiamide as a Dehydrosulfurizing Agent

T Yamamoto, A Terada, T Muramatsu…

Index: Organic Preparations and Procedures International, , vol. 26, # 5 p. 555 - 557

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Citation Number: 8

Abstract

... Although the reaction failed for the preparation of aryl isothiocyanates, the prewnt procedurc may be convenient and economical route to alkyl, arylalkyl ... General Procedure for Isothiocyanation of Alkyl Amines.- To a stirred solution of alkylamine 1 (30 rnmol) in 20 nil, of THF ... Vol. ...