e.g. Filippa Pettersson or Cancer Res. 75(6) , 1102-12, (2015) or 10.1002/anie.201600521

Ligand??Free Sonogashira Coupling Reactions with Heterogeneous Pd/C as the Catalyst

S Mori, T Yanase, S Aoyagi, Y Monguchi…

Index: Wang, Hu; Li, Li; Bai, Xing-Feng; Deng, Wen-Hui; Zheng, Zhan-Jiang; Yang, Ke-Fang; Xu, Li-Wen Green Chemistry, 2013 , vol. 15, # 9 p. 2349 - 2355

Full Text: HTML

Citation Number: 57

Abstract

... View issue TOC Volume 14, Issue 23 August 8, 2008 Pages 6994–6999. ... a phosphine ligand, and an amine is required.7 In light of recent developments towards greener chemistry, a copper ... terminal alkyne (0.6 mmol), wet-type 10 % Pd/C (4.8 mg, 0.002 mmol), Na 3 PO 4 ⋅12 H ...

Propionaldehyde Structure

Propionaldehyde

Ethyl cyanoacetate Structure

Ethyl cyanoacetate

~94%

ethyl 2-cyanopent-2-enoate Structure

ethyl 2-cyanope...

Dimethyl 4-methoxybenzylidenemalonate Structure

Dimethyl 4-meth...

Ethyl cyanoacetate Structure

Ethyl cyanoacetate

~10%

2-Propenoic acid,2-cyano-3-(4-methoxyphenyl)-, ethyl ester Structure

2-Propenoic aci...

5-Methoxy-1-indanone Structure

5-Methoxy-1-indanone

~92%

1H-Indene,2,3-dihydro-5-methoxy- Structure

1H-Indene,2,3-d...

N/A Structure

~97%

Benzene,1-ethyl-3-methoxy- Structure

Benzene,1-ethyl...

1-(4-Methoxyphenyl)ethanol Structure

1-(4-Methoxyphe...

~97%

Benzene,1-ethyl-4-methoxy- Structure

Benzene,1-ethyl...

7-Methoxy-1-tetralone Structure

7-Methoxy-1-tet...

~97%

Naphthalene,1,2,3,4-tetrahydro-6-methoxy- Structure

Naphthalene,1,2...

4-Bromoanisole Structure

4-Methoxyphenylboronic acid Structure

4-Methoxyphenyl...

~85%

4,4'-Diethylbiphenyl Structure

4,4'-Diethylbiphenyl

Dimethyl Benzylidenemalonate Structure

Dimethyl Benzyl...

Ethyl cyanoacetate Structure

Ethyl cyanoacetate

~%

Propanedioic acid,1-ethyl 3-methyl ester Structure

Propanedioic ac...

Ethyl α-cyanocinnamate Structure

Ethyl α-cyanoci...

Detail

4-Chlorophenylacetylene Structure

4-Chlorophenyla...

1-Chloro-4-iodobenzene Structure

1-Chloro-4-iodo...

~94%

Benzene,1-chloro-4-(2-phenylethynyl)- Structure

Benzene,1-chlor...

1-Chloro-4-methoxybenzene Structure

1-Chloro-4-meth...

4-Ethynylanisole Structure

4-Ethynylanisole

~97%

1-methoxy-4-[2-(4-methoxyphenyl)ethynyl]benzene Structure

1-methoxy-4-[2-...

4-Chlorophenylacetylene Structure

4-Chlorophenyla...

1-Chloro-4-iodobenzene Structure

1-Chloro-4-iodo...

~86%

Benzene, 1,1-(1,2-ethynediyl)bis(4-chloro- Structure

Benzene, 1,1-(1...

4-Chlorophenylacetylene Structure

4-Chlorophenyla...

4-Fluoroiodobenzene Structure

4-Fluoroiodobenzene

~92%

Benzene, 1,1-(1,2-ethynediyl)bis(4-chloro- Structure

Benzene, 1,1-(1...

Iodobenzene Structure

Phenylacetylene Structure

Phenylacetylene

~88%

Benzene, 1,1-(1,2-ethynediyl)bis(4-chloro- Structure

Benzene, 1,1-(1...

1-Chloro-4-methoxybenzene Structure

1-Chloro-4-meth...

Phenylacetylene-d Structure

Phenylacetylene-d

~%

Anisole, p-(phenylethynyl)- Structure

Anisole, p-(phe...

1-Chloro-4-methoxybenzene Structure

1-Chloro-4-meth...

4-Ethynyltoluene Structure

4-Ethynyltoluene

~88%

1-methoxy-4-[2-(4-methylphenyl)ethynyl]benzene Structure

1-methoxy-4-[2-...

(3,4,5-Trimethoxyphenyl)methanol Structure

(3,4,5-Trimetho...

~97%

1,2,3-Trimethoxy-5-methylbenzene Structure

1,2,3-Trimethox...

Iodobenzene Structure

Phenylacetylene Structure

Phenylacetylene

~11%

Triphenylethylene Structure

Triphenylethylene

Diphenylacetylene Structure

Diphenylacetylene

dimethyl 2-[(4-methylphenyl)methylidene]propanedioate Structure

dimethyl 2-[(4-...

Ethyl cyanoacetate Structure

Ethyl cyanoacetate

~96%

α-Cyano-4-methylbenzeneacrylic acid ethyl ester Structure

α-Cyano-4-methy...