Rapid carbohydrate protecting group manipulations assisted by microwave dielectric heating

E Söderberg, J Westman…

文献索引：Soederberg, Eva; Westman, Jacob; Oscarson, Stefan Journal of Carbohydrate Chemistry, 2001 , vol. 20, # 5 p. 397 - 410

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被引用次数: 46

摘要

The protocols for oligosaccharide synthesis are often tedious due to extended synthetic routes and reaction times. We herein describe methods assisted by microwave dielectric heating, which enable very short reaction times and high yields for the introduction and removal of eleven of the most commonly used protecting groups in carbohydrate syntheses. Several examples are reported, where solid supported reagents in combination with ...