Rapid carbohydrate protecting group manipulations assisted by microwave dielectric heating

E Söderberg, J Westman…

Index: Soederberg, Eva; Westman, Jacob; Oscarson, Stefan Journal of Carbohydrate Chemistry, 2001 , vol. 20, # 5 p. 397 - 410

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Citation Number: 46

Abstract

The protocols for oligosaccharide synthesis are often tedious due to extended synthetic routes and reaction times. We herein describe methods assisted by microwave dielectric heating, which enable very short reaction times and high yields for the introduction and removal of eleven of the most commonly used protecting groups in carbohydrate syntheses. Several examples are reported, where solid supported reagents in combination with ...