... E-mails: jackson.megiatto@asu.edu (JDM), david.schuster@nyu.edu (DIS), guldi@chemie.uni- erlangen ... The organic phase was washed with distilled water (3 × 100 mL), concentrated to a volume of 10 mL, and then stirred for 3 h with a saturated KPF 6 methanol solution to ...