Tetrahedron

Polybrominated diphenyl ethers (BDEs); preparation of reference standards and fluorinated internal analytical standards

H Liu, M Bernhardsen, A Fiksdahl

文献索引：Liu, Huiling; Bernhardsen, Monica; Fiksdahl, Anne Tetrahedron, 2006 , vol. 62, # 15 p. 3564 - 3572

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被引用次数: 23

摘要

Four new difluorinated tetra-and pentabromo BDE internal standards for GC–MS/GC–ECD analysis,,, and, have been prepared in 98–99.0% purity, mainly by coupling of the new tribromodifluorophenols () and symmetrical bromodiphenyliodonium salts (,). The four difluorinated BDEs showed promising properties as internal standards for quantitative BDE analysis. Tetra-, penta-, hexa-and hepta-brominated BDE reference standards,,, and, were ...