Tetrahedron letters

Synthesis of optically pure (S)-2-acetylthio-3-benzenepropanoic acid via enzymatic resolution

…, L You, SX Zhao, B White, JG Chen, PM Skonezny

文献索引：Zhu, Jingyang; You, Li; Zhao, Shannon X; White, Brenda; Chen, Jason G; Skonezny, Paul M Tetrahedron Letters, 2002 , vol. 43, # 42 p. 7585 - 7587

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被引用次数: 12

摘要

Please note that Internet Explorer version 8.x will not be supported as of January 1, 2016. Please refer to this blog post for more information. ... A typical procedure for enzymatic resolution: To a 100 mL three-neck round-bottom glass vessel were charged 1.0 mL 0.01 M sodium acetate or sodium phosphate buffer, pH 4.0–7.0 (5%), 19.0 mL solvent (95%), 0.254g, (1.0 mmol) racemic thioacetate ethyl esters and 0.20 g Lipozyme lipase (1%, w/v). The ...