Journal of the American Chemical Society

Diaryloxyalkane Derivatives. Some Miscellaneous Diphenoxypropanes1

FH McMillan

文献索引：McMillan Journal of the American Chemical Society, 1952 , vol. 74, p. 5229

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被引用次数: 6

摘要

ExperimentaW p, p'-Dinitro-l, 3-diphenoxypropane.-A mixture of potassium p-nitrophenoxide (35.4 g., 0.20 mole), trimethylene bromide (20.2 g., 0.10 mole) and ethylene glycol (60 ml.) was stured and heated at 130'for one hour. The cooled mixture was poured into cold water (600 ml.) giving 19.5 g.(61%) of product melting at 122-125'; after two crystallizations from ethanol it melted at 129.5-130.5". p, p'-Diamino-l, 3-diphenoxypropane.-When the above ...