An improved preparation of 3, 5-bis (trifluoromethyl) acetophenone and safety considerations in the preparation of 3, 5-bis (trifluoromethyl) phenyl Grignard reagent

JL Leazer, R Cvetovich, FR Tsay…

文献索引：Journal of Organic Chemistry, , vol. 68, # 9 p. 3695 - 3698

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被引用次数: 65

摘要

... The combined organic layer was concentrated under reduced pressure to a volume of 250 mL ... Grote, Thomas H.; Pendergrass, Kelly; Grunberg, Steven M.; Carides, Alexandra D.; Gertz, Barry J. New England Journal of Medicine (1999), 340 (3), 190-195CODEN: NEJMAG ; ISSN ...