The Journal of Organic Chemistry

General synthetic route to cycloalkylidenecycloalkanes. Reactions of. alpha.-anions of cycloalkanecarboxylic acid salts with cycloalkanones

AP Krapcho, EGE Jahngen Jr

文献索引：Krapcho,A.P.; Jahngen,E.G.E. Journal of Organic Chemistry, 1974 , vol. 39, # 12 p. 1650 - 1653

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被引用次数: 44

摘要

1650 J. Org. Chem., Vol. 39, NO. 12, 1974 Krapcho and Jahngen to remove undissolved sample. This stock solution was then stored in ice water to retard decomposition. The optical density of the stock solution was checked periodically to determine purity; experiments were never extended beyond about 4 hr. Stock solution was added to a volumetric flask by weight using a top loading analytical balance and diluted to volume with sulfuric acid solution ( ...