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举例 :可输入Filippa Pettersson 或者 Cancer Res. 75(6) , 1102-12, (2015) 或者10.1002/anie.201600521

Synthesis of anacardic acids, 6-[8 (Z), 11 (Z)-pentadecadienyl] salicylic acid and 6-[8 (Z), 11 (Z), 14-pentadecatrienyl] salicylic acid.

…, N Takeuchi, T Nishimura, T Ohta, S Tobinaga

文献索引：Satoh; Takeuchi; Nishimura; Ohta; Tobinaga Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 1 p. 18 - 22

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被引用次数: 10

摘要

11-Chloro-3-methoxy-2-undecenal was synthesized from 8-bromooctanol, and an annelation reaction with this aldehyde and ethyl acetoacetate proceeded to give the ethyl 6- (8-chlorooctyl) salicylate. Ethyl 6-(8-chlorooctyl) salicylate was converted to ethyl 6-(7- formylheptyl)-2-methoxybenzoate through the iodide after protection of the phenolic hydroxyl group. Finally, the Wittig reaction with the aldehyde and triphenylphosphonium iodides in ...

ethyl [8(Z),11(Z)-pentadecadienyl]salicylate结构式

ethyl [8(Z),11(...

~86%

2-(14-hydroxypentadeca-7,9-dien-5-yl)benzoic acid结构式

2-(14-hydroxype...

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8-溴-1-辛醇结构式

~%

2-(14-hydroxypentadeca-7,9-dien-5-yl)benzoic acid结构式

2-(14-hydroxype...

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1-溴-8-氯辛烷结构式

1-溴-8-氯辛烷

~%

2-(14-hydroxypentadeca-7,9-dien-5-yl)benzoic acid结构式

2-(14-hydroxype...

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ethyl 6-(7-formylheptyl)-2-methoxybenzoate结构式

ethyl 6-(7-form...

~%

2-(14-hydroxypentadeca-7,9-dien-5-yl)benzoic acid结构式

2-(14-hydroxype...

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11-chloro-2-undecynal结构式

11-chloro-2-und...

~%

2-(14-hydroxypentadeca-7,9-dien-5-yl)benzoic acid结构式

2-(14-hydroxype...

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11-chloro-3-methoxyacrolein结构式

11-chloro-3-met...

~%

2-(14-hydroxypentadeca-7,9-dien-5-yl)benzoic acid结构式

2-(14-hydroxype...

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11-chloro-1,1-diethoxy-2-undecyne结构式

11-chloro-1,1-d...

~%

2-(14-hydroxypentadeca-7,9-dien-5-yl)benzoic acid结构式

2-(14-hydroxype...

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ethyl 6-(8-chlorooctyl)-2-methoxybenzoate结构式

ethyl 6-(8-chlo...

~%

2-(14-hydroxypentadeca-7,9-dien-5-yl)benzoic acid结构式

2-(14-hydroxype...

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ethyl 6-(8-chlorooctyl)salicylate结构式

ethyl 6-(8-chlo...

~%

2-(14-hydroxypentadeca-7,9-dien-5-yl)benzoic acid结构式

2-(14-hydroxype...

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ethyl 6-(8-iodooctyl)-2-methoxybenzoate结构式

ethyl 6-(8-iodo...

~%

2-(14-hydroxypentadeca-7,9-dien-5-yl)benzoic acid结构式

2-(14-hydroxype...

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2-(3-丁炔氧基)四水-2H-吡喃结构式

2-(3-丁炔氧基)四水-2H-吡喃

1-碘丙烷结构式

~80%

2-hept-3-ynoxyoxane结构式

2-hept-3-ynoxyoxane

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3,4-二氢-2H-吡喃结构式

3,4-二氢-2H-吡喃

~%

2-hept-3-ynoxyoxane结构式

2-hept-3-ynoxyoxane

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烯丙基碘结构式

3-丁炔-1-醇结构式

~92%

6-庚烯-3-炔-1-醇结构式

6-庚烯-3-炔-1-醇

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2-hept-3-ynoxyoxane结构式

2-hept-3-ynoxyoxane

~90%

3-庚炔-1-醇结构式

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ethyl [8(Z),11(Z),14-pentadecatrienyl]salicylate结构式

ethyl [8(Z),11(...

~89%

Anacardic Acid triene结构式

Anacardic Acid ...

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8-溴-1-辛醇结构式

~%

Anacardic Acid triene结构式

Anacardic Acid ...

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1-溴-8-氯辛烷结构式

1-溴-8-氯辛烷

~%

Anacardic Acid triene结构式

Anacardic Acid ...

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ethyl 6-(7-formylheptyl)-2-methoxybenzoate结构式

ethyl 6-(7-form...

~%

Anacardic Acid triene结构式

Anacardic Acid ...

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ethyl 2-methoxy-6-[8(Z),11(Z),14-pentadecatrienyl]benzoate结构式

ethyl 2-methoxy...

~%

Anacardic Acid triene结构式

Anacardic Acid ...

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11-chloro-2-undecynal结构式

11-chloro-2-und...

~%

Anacardic Acid triene结构式

Anacardic Acid ...

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11-chloro-3-methoxyacrolein结构式

11-chloro-3-met...

~%

Anacardic Acid triene结构式

Anacardic Acid ...

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11-chloro-1,1-diethoxy-2-undecyne结构式

11-chloro-1,1-d...

~%

Anacardic Acid triene结构式

Anacardic Acid ...

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ethyl 6-(8-chlorooctyl)-2-methoxybenzoate结构式

ethyl 6-(8-chlo...

~%

Anacardic Acid triene结构式

Anacardic Acid ...

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ethyl 6-(8-chlorooctyl)salicylate结构式

ethyl 6-(8-chlo...

~%

Anacardic Acid triene结构式

Anacardic Acid ...

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ethyl 6-(8-iodooctyl)-2-methoxybenzoate结构式

ethyl 6-(8-iodo...

~%

Anacardic Acid triene结构式

Anacardic Acid ...

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