Optimization of the synthesis of 2-phenyl-1, 2, 3-triazole

GF Myachina, TG Ermakova, NP Kuznetsova…

文献索引：Myachina; Ermakova; Kuznetsova; Sultangareev; Larina; Klyba; Suchanov; Trofimov Chemistry of Heterocyclic Compounds, 2010 , vol. 46, # 1 p. 79 - 81

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被引用次数: 2

摘要

The synthesis of 2-phenyl-1, 2, 3-triazole by the cyclization of glyoxal phenylosazone in high- boiling solvents in the presence of copper triflate catalyst has been optimized. The structure of the product was confirmed by data of IR, 1 H, 13 C, and 15 N NMR spectroscopy, mass spectrometry, and elemental analysis.