Synthesis of polyfunctional aromatic ring systems (phloroglucide analogs) under microwave irradiation

A Khalafi??Nezhad, MNS Rad…

文献索引：Khalafi-Nezhad, Ali; Rad, Mohammad Navid Soltani; Hakimelahi, Gholam Hossein Helvetica Chimica Acta, 2003 , vol. 86, # 7 p. 2396 - 2403

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被引用次数: 37

摘要

Abstract An efficient and rapid synthesis of phloroglucide analogs under microwave irradiation is described. The solid-phase condensation reaction of the 4-halo-2, 6-bis (hydroxymethyl) phenols 1a, b with other substituted phenols in the presence of ZnCl 2 afforded the target molecules in much higher yields than by classical solution-phase synthesis and allowed us to prepare new phloroglucide analogs possessing sensitive ...