" Yield for method A refers to two-step process from acid chloride to thioamide; method B is for one-step transformation from amide to thioamide. Mp 73-75" C. Bp 100" C (150 pm). Bp 90" C (150 pm). e Bp 100" C (100 pm). amenable to this process were investigated as well as the conditions required to efficiently invoke the extrusion. This led to the development of a reagent which served the dual role of base to abstract the a-proton and thiophile to assist ...
[Aissa, Christophe; Riveiros, Ricardo; Ragot, Jacques; Fuerstner, Alois Journal of the American Chemical Society, 2003 , vol. 125, # 50 p. 15512 - 15520]
