Journal of heterocyclic chemistry

An unexpected preparation of 4??oxo??2H??1, 3??benzothiazines

FA Golec, P Lee, JR Lloyd

文献索引：Golec, Frederick A.; Lee, Paul; Lloyd, John R. Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1755 - 1756

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被引用次数: 1

摘要

Abstract Treatment of compound N, N-(dithiobis (3-chloro-2, 1-phenylene) dicarbonylbis (N- cyclopentylglycine) diethyl ester (3) with methanolic sodium hydroxide does not produce the expected hydrolysis product N, N-(dithiobis-(3-chloro-2, 1-phenylene) dicarbonylbis (N- cylcopentylglycine)(4) but yields a mixture of compounds 8-chloro-3-cyclopentyl-3, 4-dihydro- 4-oxo-2H-1, 3-benzothiazine-2-carboxylic acid (6) and N-(3-chloro-2-mercaptobenzoyl)-N ...