Aryllithiums with Increasing Steric Crowding and Lipophilicity Prepared from Chlorides in Diethyl Ether. The First Directly Prepared Room-Temperature-Stable …

…, BR Steele, M Micha-Screttas, GA Heropoulos

文献索引：Screttas, Constantinos G.; Steele, Barry R.; Micha-Screttas, Maria; Heropoulos, Georgios A. Organic Letters, 2012 , vol. 14, # 22 p. 5680 - 5683

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被引用次数: 10

摘要

A convenient procedure has been developed for the preparation of synthetically useful, room-temperature-stable aryllithiums starting from aryl chlorides and lithium metal. The method provides a route to aryllithiums which have previously not been accessible cleanly or could only be prepared by using more expensive starting materials.

95-72-7

2-氯-1,4-二甲基苯

~97%

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~83%

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~53%

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~84%

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~71%

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~99%

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~93%

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~12%

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~97%

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~36%

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~79%

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~95%

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~76%

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~61%

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~98%

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~57%

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~40%

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Syntheses of aryl glyoxylate. I. The reaction of alkyl dichl...

[Itoh, Osamu; Nagata, Takayoshi; Nomura, Isamu; Takanaga, Tetsuya; Sugita, Toshio; Ichikawa, Katsuhiko Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 810 - 814]