Organic disulfides and related substances. XXI. Sulfuryl chloride in the preparation of thiosulfonates from disulfides

JD Buckman, M Bellas, HK Kim…

文献索引：Buckman,J.D. et al. Journal of Organic Chemistry, 1967 , vol. 32, p. 1626 - 1627

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被引用次数: 18

摘要

Department of Chemistry, Vanderbilt University, Nashville, Tenneasee 37903 symmetrical thiol sulfonate^.^ Since sulfuryl chloride has been used to convert disulfides and thiols to sulfenyl chloride^,^ key intermediates in the Douglass-Farah reaction, 2 and since it is very easily handled, it presented a useful alternative to chlorine in the Douglass-Farah synthesis; there is also the prospect of greater flexibility in conditions than with a gas, and of useful ...