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Journal of the American Chemical Society

The condensation of some tertiary aryl substituted carbinols with phenol in the presence of aluminum chloride

LH Welsh, NL Drake

文献索引:Welsh; Drake Journal of the American Chemical Society, 1938 , vol. 60, p. 59,61

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被引用次数: 8

摘要

Aqueous Ammonium Hydroxide.-The aluminum amalgam was prepared by adding small pieces of aluminum foil to a dilute solution of mercuric chloride. A vigorous reaction took place and after standing a few minutes, the amalgam was poured upon a Buchner funnel and well washed with water and then with alcohol. This amalgam must be used immediately because of its great reactivity. Twenty grams of this aluminum amalgam was covered with ...