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The Journal of Organic Chemistry

New procedures for preparation of potassium 3-aminopropylamide

T Kimmel, D Becker

文献索引:Kimmel, T.; Becker, D. Journal of Organic Chemistry, 1984 , vol. 49, # 13 p. 2494 - 2496

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被引用次数: 29

摘要

" Products were identified by comparison with authentic samples and/or from spectra. bThe ratio of product to starting material is> 982 according to GC analysis. in ammonia, ammonia gas was bubbled into a stirred mixture of molten potassium and 193-propanediamine at 80 OC. That KAPA was formed was demonstrated by isomerizing acetylenes (see Table I). We do not know whether ammonia plays a role only as solvent for potas-sium or whether it ...