Journal of the American Chemical Society

Organic Reactions with Boron Fluoride. 1 XIX. Condensation of Cyclopropane and Olefins with Acids

TB Dorris, FJ Sowa

文献索引：Dorris; Sowa Journal of the American Chemical Society, 1938 , vol. 60, p. 358

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被引用次数: 9

摘要

Procedure.-The apparatus consisted of a three-necked round-bottomed flask containing an inlet and outlet tube and connected with a sealed-in~ tirrer.~ The outlet was connected to a mercury sealed pressure regulator. Ordinarily, an equivalent amount of boron fluoride was added to a suspension of the acid in a solvent. The unsaturated hydrocarbon [propylene, a mixture of butylenes (80% iso, 20% alpha-and beta-), or cyclopropane] vigorous stirring. ...