Formation of the crossed product 1, 4-disubstituted 2, 3, 5, 6, 11-pentaoxabicyclo [5.3. 1] undecane from a mixture of two kinds of ozonides in the presence of an acid …

M Miura, M Nojima, S Kusabayashi…

文献索引：Miura,M.; Nojima,M.; Kusabayashi,S. Journal of the American Chemical Society, 1981 , vol. 103, p. 1789

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被引用次数: 11

摘要

Method B. To a stirred solution of 0.52 g (1.08 mmol) of 13 in 2 mL of hexamethylphosphorictriamide, at 10 OC, was added 0.33 g (2.7 mmol) of sodium 2, 2, 2- trifluoroethoxide in 2 mL of the same solvent. Immediately after mixing the NMR spectral ...