Molecular Spoked Wheels: Synthesis and Self??Assembly Studies on Rigid Nanoscale 2D Objects

AV Aggarwal, SS Jester, SM Taheri…

文献索引：Aggarwal, A. Vikas; Jester, Stefan-S.; Taheri, Sara Mehdizadeh; Foerster, Stephan; Hoeger, Sigurd Chemistry - A European Journal, 2013 , vol. 19, # 14 p. 4480 - 4495

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被引用次数: 9

摘要

Abstract We present the efficient synthesis of a new molecular spoked-wheel structure (MSW- 3). Two derivatives with diameters of approximately 4 nm have been prepared. By highlighting the importance of pseudo-high-dilution conditions during cyclization, we were able to access the compounds on a several hundred milligram scale. In addition to the standard characterization (NMR spectroscopy, MS), we describe a detailed investigation ...