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Condensations of Esters by Diisopropylaminomagnesium Bromide and Certain Related Reagents

FC Frostick, CR Hauser

文献索引:Frostick; Hauser Journal of the American Chemical Society, 1949 , vol. 71, p. 1351,1352

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被引用次数: 34

摘要

1350 FREDERICK c. FROSTICK, JR., AND CHARLES R. HAUSER ... (1.89 g.) were ebtained. These were recrystallized from an eq2al mixture of benzene and alcohol, m. p. 155.0- 155.5 . Anal. Calcd. for CtaHn: C. 94.20; H, 5.80. Found: C, 94.57; H, 5.67. (B) 3-(3-Xeny1)-Az-cyclohexenone (111) was prepared as described above. A 40-ml. dry ether solution of the substance (17.6 9.) was added to a 40-ml. dry ether solution of 4-xenyllithium, ...