tert-Butyl (2-hydroxy-2-phenylethyl)carbamate

Modify Date: 2024-01-10 17:42:28

tert-Butyl (2-hydroxy-2-phenylethyl)carbamate Structure
tert-Butyl (2-hydroxy-2-phenylethyl)carbamate structure
Common Name tert-Butyl (2-hydroxy-2-phenylethyl)carbamate
CAS Number 67341-07-5 Molecular Weight 237.295
Density 1.1±0.1 g/cm3 Boiling Point 389.4±35.0 °C at 760 mmHg
Molecular Formula C13H19NO3 Melting Point N/A
MSDS N/A Flash Point 189.3±25.9 °C

 Names

Name tert-butyl N-(2-hydroxy-2-phenylethyl)carbamate
Synonym More Synonyms

 Chemical & Physical Properties

Density 1.1±0.1 g/cm3
Boiling Point 389.4±35.0 °C at 760 mmHg
Molecular Formula C13H19NO3
Molecular Weight 237.295
Flash Point 189.3±25.9 °C
Exact Mass 237.136490
PSA 62.05000
LogP 2.33
Vapour Pressure 0.0±0.9 mmHg at 25°C
Index of Refraction 1.523

 Safety Information

HS Code 2924299090

 Synthetic Route

~99%

tert-Butyl (2-hydroxy-2-phenylethyl)carbamate Structure

tert-Butyl (2-h...

CAS#:67341-07-5

Literature: F. HOFFMANN-LA ROCHE AG; LIU, Wenjian; LUK, Kin-Chun Thomas; ZHANG, Xiaohu Patent: WO2012/98068 A1, 2012 ; Location in patent: Page/Page column 20-21 ;

~90%

tert-Butyl (2-hydroxy-2-phenylethyl)carbamate Structure

tert-Butyl (2-h...

CAS#:67341-07-5

Literature: Chandrasekhar; Chandraiah; Raji Reddy; Venkat Reddy Chemistry Letters, 2000 , # 7 p. 780 - 781

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tert-Butyl (2-hydroxy-2-phenylethyl)carbamate Structure

tert-Butyl (2-h...

CAS#:67341-07-5

Literature: Sankyo Company, Limited Patent: US4699905 A1, 1987 ; US 4699905 A

~84%

tert-Butyl (2-hydroxy-2-phenylethyl)carbamate Structure

tert-Butyl (2-h...

CAS#:67341-07-5

Literature: Masruri; Willis, Anthony C.; McLeod, Malcolm D. Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8480 - 8491

~94%

tert-Butyl (2-hydroxy-2-phenylethyl)carbamate Structure

tert-Butyl (2-h...

CAS#:67341-07-5

Literature: Ishizuka, Tadao; Kunieda, Takehisa Tetrahedron Letters, 1987 , vol. 28, # 36 p. 4185 - 4188

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tert-Butyl (2-hydroxy-2-phenylethyl)carbamate Structure

tert-Butyl (2-h...

CAS#:67341-07-5

Detail
Literature: O'Brien, Peter; Osborne, Simon A.; Parker, Daniel D. Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 16 p. 2519 - 2526

~%

tert-Butyl (2-hydroxy-2-phenylethyl)carbamate Structure

tert-Butyl (2-h...

CAS#:67341-07-5

Literature: Masruri; Willis, Anthony C.; McLeod, Malcolm D. Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8480 - 8491

~%

tert-Butyl (2-hydroxy-2-phenylethyl)carbamate Structure

tert-Butyl (2-h...

CAS#:67341-07-5

Literature: Herranz,E. et al. Journal of the American Chemical Society, 1978 , vol. 100, p. 3596 - 3598

 Customs

HS Code 2924299090
Summary 2924299090. other cyclic amides (including cyclic carbamates) and their derivatives; salts thereof. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:30.0%

 Synonyms

Carbamic acid, N-(2-hydroxy-2-phenylethyl)-, 1,1-dimethylethyl ester
N-Boc-DL-Phenylglycinol
AC-7089
2-Methyl-2-propanyl (2-hydroxy-2-phenylethyl)carbamate
tert-Butyl (2-hydroxy-2-phenylethyl)carbamate
N-Boc-2-hydroxy-2-phenylethylamine