Improved preparative route toward 3-arylcyclopropenes
WM Sherrill, R Kim, M Rubin
Index: Sherrill, William M.; Kim, Ryan; Rubin, Michael Tetrahedron, 2008 , vol. 64, # 37 p. 8610 - 8617
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Citation Number: 26
Abstract
A convenient preparative protocol for the synthesis of various 3-arylcyclopropenes in a multigram scale is disclosed. Optimization of the reaction conditions and isolation procedures allowed for significant improvement of the chemical yields of these strained products. The described protocol was used for efficient preparation of a series of 3-methyl-3- arylcyclopropenes possessing different substituents in the aromatic ring. The effect of ...
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