Facile anhydride synthesis using trichlorotrifluoroacetone hydrate

S Abdel-Baky, RW Giese

Index: Abdel-Baky, Samy; Giese, Roger W. Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3390 - 3391

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Citation Number: 20

Abstract

Infrared spectra were taken on Perkin-Elmer Model X99 spectrophotometer and the absorptions are reported in wave numbers (ad). Mass spectra were obtained on a Nuclide 12-90-G instrument. Melting pointa were determined on a Thomas-Hoover capillary melting point apparatus and are uncorrected. Elemental analysis was performed by MultiChem Laboratories. l, l, l-Tri-chloro-3, 3, 3-trifluoroacetone was obtained from Fluke Chemical