An efficient and convergent synthesis of the potent and selective H 3 antagonist ABT-239
YY Ku, YM Pu, T Grieme, P Sharma, AV Bhatia…
Index: Tetrahedron, , vol. 62, # 18 p. 4584 - 4589
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Citation Number: 17
Abstract
... Tetrahedron. ... mixture as a solid in portions maintaining the reaction temperature below 30 °C. The reaction mixture was then stirred at 62 °C for 4 h ... The reaction mixture was concentrated to one-fourth of the original volume, and methyl tert-butyl ether (200 mL) was added to the ...
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