Allergenic. alpha.-methylene-. gamma.-lactones. General method for the preparation of. beta.-acetoxy-and. beta.-hydroxy-. alpha.-methylene-. gamma.-butyrolactones …
JP Corbet, C Benezra
Index: Corbet, Jean-Pierre; Benezra Claude Journal of Organic Chemistry, 1981 , vol. 46, # 6 p. 1141 - 1147
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Citation Number: 26
Abstract
Results and Discussion Synthesis of 8-Hydroxy-a-methylene-7-butyrolactones. When this work was started, only one preparation of tulipalin B (1, P-hydroxy-a-methylene-y- butyrolactone) was in the literature,'and it consisted of the allylic oxidation of a-methylene-y- butyrolactone (3) with SeOz and gave poor yields (Scheme I). Recent19 this compound was prepared by another route. Since 1 and its derivatives are allylic alcohols, it seemed ...
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