Gas chromatography-mass spectrometry of trimethylsilylated imino derivatives of alanine.

K Kawashiro, S Morimoto, H Yoshida

Index: Kawashiro, Katsuhiro; Morimoto, Shiro; Yoshida, Hideyuki Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 7 p. 1903 - 1912

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Citation Number: 7

Abstract

Trimethylsilylation of seven imino derivatives of alanine with N, O-bis (trimethylsilyl) trifluoroacetamide in acetonitrile was studied. The imino derivatives include 2, 2′- iminodipropionitrile (1), 2, 2′-iminodipropionamide (2), 2, 2′-iminodipropionic acid (3), 2- (1-cyanoethylamino) propionamide (4), 2-(1-cyanoethylamino) propionic acid (5), 2-(1- carbamoylethylamino) propionic acid (6), and 3, 5-dimethyl-2, 6-piperazinedione (7). The ...