2, 3-Dimethylbutanal and 2-Ethyl-3-methylbutanal

RA Barnes, WM Budde

Index: Barnes; Budde Journal of the American Chemical Society, 1946 , vol. 68, p. 2339

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Citation Number: 15

Abstract

Sulfuric acid hydrolysis of m-nitrophenylthiorrcet- morpholide gave a 22% yield of m-nitrophenylacetic acid which melted at 117-119" after recrystallizatioa from water; its m. p. is variously reported*8 as 117 to 120 . Use of Other Amines.-The standard procedure de- scribed for morpholine and styrene was used in all the comparative runs made with other amines and styrene. In only four cases were the thioamides isolated and puri- fied. The results are summarized in ...