An efficient and safe procedure for the large-scale Pd-catalyzed hydrazonation of aromatic chlorides using buchwald technology

CC Mauger, GA Mignani

Index: Organic Process Research and Development, , vol. 8, # 6 p. 1065 - 1071

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Citation Number: 32

Abstract

... Layers were separated, and the arylhydrazone was allowed to crystallize in the organic layer at a ... The standard procedure is applied to an 18-L glass reactor linked to a Raman ... Indeed, this process monitoring enables us to determine the reaction completion with optimization of ...

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