Synthesis of 5-phenyl-2, 3, 4, 5-tetrahydro-1, 4-benzoxazepines and corresponding 3-ones
GN Walker, RT Smith
Index: Walker,G.N.; Smith,R.T. Journal of Organic Chemistry, 1971 , vol. 36, p. 305 - 308
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Citation Number: 34
Abstract
Preliminary, unsuccessful attempts to obtain di-and tetrahydro-5-phenyl-7-chloro-l14- benaoxaeepines through reactions of derivatives of 2-hydroxy-5-chlorobeneophenone oxime (2a-d) and of 2-(carboxymeth-oxy)-5-chlorobenzophenone and benehydrol (5-8) are described. A successful route to the title compounds differing from existing methods for synthesis of (hydro) 1, 4-beneoxaaepines was found involving novel preparation of o- ...
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